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on peut augmenter le flux dans la cellule d'ablation jusqu ,
Il n'y a de nouveau aucun changement à effectuer. Les paramètres (les mêmes que ci-dessous) sont adéquats pour les analyses de minéraux et inclusions fluides ,
Cette fenêtre permet de rentrer des équations d'interférence et ainsi d'avoir de meilleurs résultats sur les éléments présentant ce type de problème. Voir avec le responsable ce qu'il est possible de faire suivant son set d'éléments. Puis cliquer sur Ok La fenêtre suivante permet de choisir le mode d'acquisition de l'ICP-MS. Pour le couplage ablation laser et ICP-MS, l'acquisition qui permet d'obtenir des résultats est Time Resolved Analysis ,
Plus le temps est important et plus l'ICP-MS va être sensible Sur les majeurs, utiliser des temps plus courts (éviter la saturation du détecteur) : 0.005 à 0.010 s. Sur les mineurs, utiliser des temps plus long 0.010 à 0.100s. Il faut également faire attention au temps d'acquisition de l'ensemble des éléments analysés (noté Sampling dans cette fenêtre) Pour les inclusions fluides ,
U ou He.U d) Acquisition des données Cliquer sur AcquireData puis Main Panel? La fenêtre où l'on va pouvoir suivre en direct l'acquisition s'ouvre ,
D:\ICPMS\1\DATA (chemin par défaut) Rentrer ensuite la date dans Data Batch sous forme année/mois/jour, puis rentrer le nom de l'échantillon dans Data File Name ,
Pour arrêter l'ablation, cliquer sur stop Bouton Start/Stop Nombre de tirs Fréquence Taille de l'ablation Click droit dans cette fenêtre pour afficher ce menu déroulant ,
(date) SURTOUT Cela permettra de garder des traces de toutes les analyses effectuées par LA-ICP- MS et en cas de problème de remonter plus facilement à la source. b) Modification des paramètres pour améliorer le signal Pour cette opération, il n'est pas nécessaire d'avoir accès à tous les paramètres du plasma, p.1 ,
le troisième onglet permet de choisir les masses que l'on va observer lorsque l'on modifie les paramètres (Onglet : Acq. Parameters) ,