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A. Iii and .. Protocole-expérimental-d-'étude-de-la-pyrolyse-au-four-À-image-vertical, 15 1. Préparation des échantillons, p.15

A. Viii and .. Gc-ms-fid, Chromatogrammes réalisées sur les matières volatiles en, p.45

. Allumer-la-lampe-du-four-À-image, Allumer le boîtier Brooks ainsi que tous les appareils (ordinateur, moteur du four, freins)

À. La-fin-de-l-'expérience,-fermer-le and . Lampe, Monter le four jusqu'à sa position la plus haute, enlever les pièces céramiques

. Fermer-le-sac-de-gaz, Désassembler le réacteur et les différents éléments du montage. Pour le condenseur, fermer les deux extrémités à l'aide des bouchons

. Dans-le-cas-d, une pyrolyse incomplète, la biomasse et le charbon sont séparés par grattage à l'aide d'une lame. Après séparation, ou dans le cas d'une pyrolyse totale

L. Gaz-récupérés-dans-le-sac-d, échantillonnage sont analysés par chromatographie en phase gazeuse. Les gaz permanents sont analysés par micro-GC, où le sac de gaz est directement relié à l'appareil pour prélèvement. Les hydrocarbures légers sont analysés par GC-FID, où un volume (250 µL) est prélevé à l'aide d'une seringue à travers le septum du sac