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15 1. Préparation des échantillons, p.15 ,
Chromatogrammes réalisées sur les matières volatiles en, p.45 ,
Allumer le boîtier Brooks ainsi que tous les appareils (ordinateur, moteur du four, freins) ,
Monter le four jusqu'à sa position la plus haute, enlever les pièces céramiques ,
Désassembler le réacteur et les différents éléments du montage. Pour le condenseur, fermer les deux extrémités à l'aide des bouchons ,
une pyrolyse incomplète, la biomasse et le charbon sont séparés par grattage à l'aide d'une lame. Après séparation, ou dans le cas d'une pyrolyse totale ,
échantillonnage sont analysés par chromatographie en phase gazeuse. Les gaz permanents sont analysés par micro-GC, où le sac de gaz est directement relié à l'appareil pour prélèvement. Les hydrocarbures légers sont analysés par GC-FID, où un volume (250 µL) est prélevé à l'aide d'une seringue à travers le septum du sac ,