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Synthesis of Methyl 3-Azidothieno[2,3-b]pyridine-2-carboxylates and Application of the Huisgen Reaction

Abstract : The preparation of new substituted methyl 3-azidothieno[2,3-b]pyridine carboxylates by azotization of methyl 3-aminothieno[2,3-b]pyridine and subsequent treatment with sodium azide is described. Via Huisgen's 1,3-dipolar cycloaddition between substituted alkynes and the prepared azides, methyl 1,2,3-triazolo-thieno[2,3-b]pyridine carboxylates have been obtained.
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https://hal.univ-lorraine.fr/hal-01494560
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Submitted on : Thursday, March 23, 2017 - 4:19:54 PM
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Wafaa Chaouni, Mina Aadil, Ahmed Djellal, Gilbert Kirsch. Synthesis of Methyl 3-Azidothieno[2,3-b]pyridine-2-carboxylates and Application of the Huisgen Reaction. Zeitschrift fur Naturforschung B, Verlag der Zeitschrift Fuer Naturforschung, 2014, 69 (5), pp.509-518. ⟨10.5560/ZNB.2014-3320⟩. ⟨hal-01494560⟩

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