Facile Synthesis of Hydrazine Derivatives of 5H-Pyrrolo[3,4-b]pyrazine and 1H-Pyrrolo[3,4-b]quinoxaline - Université de Lorraine Accéder directement au contenu
Article Dans Une Revue Synthesis: Journal of Synthetic Organic Chemistry Année : 2013

Facile Synthesis of Hydrazine Derivatives of 5H-Pyrrolo[3,4-b]pyrazine and 1H-Pyrrolo[3,4-b]quinoxaline

Résumé

A convenient and efficient route for the chemoselective synthesis of carbohydrazide, arenesulfonylhydrazide, and thiosemicarbazone derivatives of 5H-pyrrolo[3,4-b]pyrazine and 1H-pyrrolo[3,4-b]quinoxaline from the corresponding dinitriles and substituted hydrazines was elaborated. The synthesis of starting pyrazine-2,3-dicarbonitrile was sufficiently improved by using concentrated HCl as a catalyst.
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Dates et versions

hal-01498208 , version 1 (29-03-2017)

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Olga V. Hordiyenko, Igor V. Rudenko, Irina A. Zamkova, Oleksandr V. Denisenko, Angelina V. Biitseva, et al.. Facile Synthesis of Hydrazine Derivatives of 5H-Pyrrolo[3,4-b]pyrazine and 1H-Pyrrolo[3,4-b]quinoxaline. Synthesis: Journal of Synthetic Organic Chemistry, 2013, 45 (24), pp.3375-3382. ⟨10.1055/s-0033-1340042⟩. ⟨hal-01498208⟩
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