Microwave-assisted synthesis of zinc 5-(4-carboxyphenyl)-10,15,20-triphenylporphyrin and zinc 5-(4-carboxyphenyl)-10,15,20-triphenylchlorin

Abstract : The microwave-assisted synthesis of zinc 5-(4-carboxyphenyl)-10,15,20-triphenylporphyrin and zinc 5-(4-carboxyphenyl)-10,15,20-triphenylchlrorin are described and compared to classic conditions of synthesis in terms of time of reaction and yields obtained. The new experimental protocols are easy to implement required small amounts of reagents and solvents and lead to short reaction times. All compounds have been characterized by H-1 NMR, MS and spectroscopic techniques.
Type de document :
Article dans une revue
Journal of Porphyrins and Phthalocyanines, World Scientific Publishing, 2015, 19 (4), pp.595-600. 〈10.1142/S1088424614500953〉
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https://hal.univ-lorraine.fr/hal-01267219
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Soumis le : jeudi 4 février 2016 - 10:10:54
Dernière modification le : vendredi 16 février 2018 - 11:08:06

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Rima Chouikrat, Aymeric Champion, Régis Vanderesse, Céline Frochot, Albert Moussaron. Microwave-assisted synthesis of zinc 5-(4-carboxyphenyl)-10,15,20-triphenylporphyrin and zinc 5-(4-carboxyphenyl)-10,15,20-triphenylchlorin. Journal of Porphyrins and Phthalocyanines, World Scientific Publishing, 2015, 19 (4), pp.595-600. 〈10.1142/S1088424614500953〉. 〈hal-01267219〉

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