Microwave-Assisted Functionalization of Single-Wall Carbon Nanotubes Through Diazonium - Université de Lorraine
Journal Articles Journal of Nanoscience and Nanotechnology Year : 2007

Microwave-Assisted Functionalization of Single-Wall Carbon Nanotubes Through Diazonium

Jie Liu
  • Function : Author
  • PersonId : 1012435
Mireia Rodriguez I Zubiri
Brigitte Vigolo
Yves Fort
  • Function : Author
Edward Mcrae
  • Function : Author

Abstract

Single-wall carbon nanotubes (SWNTs) have been functionalized by a diazonium method through both a classical thermal reaction and a microwave-assisted reaction. The functionalized SWNTs have been characterized by nIR-Vis-UV absorption spectroscopy, Raman spectroscopy, and thermal gravimetric analysis. The results show that SWNTs are covalently functionalized through both reactions and that the microwave-assisted reaction is more rapid. Moreover, optimal choice of the reaction time can prevent the microwave irradiation from the adverse effect of subsequently removing the functional groups on the SWNT surface.
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Dates and versions

hal-01849011 , version 1 (25-07-2018)

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Jie Liu, Mireia Rodriguez I Zubiri, Brigitte Vigolo, M. Dossot, Bernard Humbert, et al.. Microwave-Assisted Functionalization of Single-Wall Carbon Nanotubes Through Diazonium. Journal of Nanoscience and Nanotechnology, 2007, 7 (10), pp.3519 - 3523. ⟨10.1166/jnn.2007.819⟩. ⟨hal-01849011⟩
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