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Accurate electron channeling contrast analysis of a low angle sub-grain boundary

Abstract : High resolution selected area channeling pattern (HR-SACP) assisted accurate electron channeling contrast imaging (A-ECCI) was used to unambiguously characterize the structure of a low angle grain boundary in an interstitial-free-steel. The boundary dislocations were characterized using TEM-style contrast analysis. The boundary was determined to be tilt in nature with a misorientation angle of 0.13 degrees consistent with the HR-SACP measurements. The results were verified using high accuracy electron backscatter diffraction (EBSD), confirming the approach as a discriminating tool for assessing low angle boundaries.
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https://hal.univ-lorraine.fr/hal-01513866
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Haithem Mansour, M. A. Crimp, Nathalie Gey, Nabila Maloufi. Accurate electron channeling contrast analysis of a low angle sub-grain boundary. Scripta Materialia, Elsevier, 2015, 109, pp.76-79. ⟨10.1016/j.scriptamat.2015.07.023⟩. ⟨hal-01513866⟩

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